Information card for entry 4313741

Structure parameters

• Formula: C2.91 H8.91 Ge0.73 N1.45 O4.64 V1.27
• Calculated formula: C2.90909 H8.72727 Ge0.727273 N1.45455 O4.63636 V1.27273
• Title of publication: Vanadogermanate Cluster Anions
• Authors of publication: T. Whitfield; X. Wang; A. J. Jacobson
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 3728 - 3733
• a: 14.995 ± 0.0007 Å
• b: 14.995 ± 0.0007 Å
• c: 18.4077 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4139 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 134
• Hermann-Mauguin space group symbol: P 42/n n m :2
• Hall space group symbol: -P 4ac 2bc
• Residual factor for all reflections: 0.0911
• Residual factor for significantly intense reflections: 0.0493
• Weighted residual factors for significantly intense reflections: 0.1339
• Weighted residual factors for all reflections included in the refinement: 0.1504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No