Information card for entry 4313926

Structure parameters

• Formula: C20 H39 B F3 N7 O4 P2 Ru S
• Calculated formula: C20 H39 B F3 N7 O4 P2 Ru S
• Title of publication: Octahedral Ru(II) Amido Complexes TpRu(L)(L')(NHR) (Tp = Hydridotris(pyrazolyl)borate; L = L' = P(OMe)3 or PMe3 or L = CO and L' = PPh3; R = H, Ph, ortBu): Synthesis, Characterization, and Reactions with Weakly Acidic C-H Bonds
• Authors of publication: David Conner; K. N. Jayaprakash; Michael B. Wells; Selena Manzer; T. Brent Gunnoe; Paul D. Boyle
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 4759 - 4772
• a: 9.4716 ± 0.0006 Å
• b: 11.6028 ± 0.0009 Å
• c: 14.3274 ± 0.0016 Å
• α: 88.195 ± 0.008°
• β: 82.61 ± 0.009°
• γ: 74.679 ± 0.006°
• Cell volume: 1506 ± 0.2 ų
• Cell temperature: 148 K
• Ambient diffraction temperature: 148 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.035
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for all reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.045
• Goodness-of-fit parameter for significantly intense reflections: 1.64
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MolybdenumKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No