Information card for entry 4313928

Structure parameters

• Formula: C36 H30 B N6 O P Ru
• Calculated formula: C36 H30 B N6 O P Ru
• Title of publication: Octahedral Ru(II) Amido Complexes TpRu(L)(L')(NHR) (Tp = Hydridotris(pyrazolyl)borate; L = L' = P(OMe)3 or PMe3 or L = CO and L' = PPh3; R = H, Ph, ortBu): Synthesis, Characterization, and Reactions with Weakly Acidic C-H Bonds
• Authors of publication: David Conner; K. N. Jayaprakash; Michael B. Wells; Selena Manzer; T. Brent Gunnoe; Paul D. Boyle
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 4759 - 4772
• a: 10.9799 ± 0.0008 Å
• b: 17.0455 ± 0.0018 Å
• c: 19.0928 ± 0.0019 Å
• α: 110.135 ± 0.009°
• β: 104.279 ± 0.007°
• γ: 93.514 ± 0.009°
• Cell volume: 3209.1 ± 0.6 ų
• Cell temperature: 148 K
• Ambient diffraction temperature: 148 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.028
• Residual factor for significantly intense reflections: 0.027
• Weighted residual factors for all reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.033
• Goodness-of-fit parameter for significantly intense reflections: 1.62
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MolybdenumKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No