Information card for entry 4314020

Structure parameters

• Formula: C60 H50 Cl2 N4 P3 V
• Calculated formula: C56.48 H45 Cl2 N3 P3 V
• Title of publication: Synthesis and Characterization of Vanadium(V)-Phosphinimide Complexes
• Authors of publication: Sarah B. Hawkeswood; Douglas W. Stephan
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 5429 - 5433
• a: 13.646 ± 0.006 Å
• b: 13.646 ± 0.006 Å
• c: 47.73 ± 0.03 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 7697 ± 7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0758
• Residual factor for significantly intense reflections: 0.0365
• Weighted residual factors for significantly intense reflections: 0.0974
• Weighted residual factors for all reflections included in the refinement: 0.1217
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No