Information card for entry 4314038

Structure parameters

• Formula: C34 H60 B Li O P2
• Calculated formula: C34 H60 B Li O P2
• Title of publication: Bis(phosphino)borates: A New Family of Monoanionic Chelating Phosphine Ligands
• Authors of publication: J. Christopher Thomas; Jonas C. Peters
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 5055 - 5073
• a: 16.295 ± 0.003 Å
• b: 12.898 ± 0.002 Å
• c: 17.47 ± 0.003 Å
• α: 90°
• β: 105.48 ± 0.003°
• γ: 90°
• Cell volume: 3538.5 ± 1 ų
• Cell temperature: 98 ± 2 K
• Ambient diffraction temperature: 98 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0795
• Residual factor for significantly intense reflections: 0.0517
• Weighted residual factors for significantly intense reflections: 0.0896
• Weighted residual factors for all reflections included in the refinement: 0.0952
• Goodness-of-fit parameter for all reflections included in the refinement: 1.879
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No