Information card for entry 4314079

Structure parameters

• Formula: C32 H26 Cl2 N10 O9 Pd2
• Calculated formula: C32 H24 Cl2 N10 O9 Pd2
• Title of publication: Design and Synthesis of a New Binucleating Ligand via Cobalt-Promoted C-N Bond Fusion Reaction. Ligand Isolation and Its Coordination to Nickel, Palladium, and Platinum
• Authors of publication: Kunal K. Kamar; Srijit Das; Chen-Hsiung Hung; Alfonso Castiñeiras; Michael D. Kuz'min; Conrado Rillo; Juan Bartolomé; Sreebrata Goswami
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 5367 - 5375
• a: 12.5546 ± 0.0009 Å
• b: 14.4884 ± 0.0011 Å
• c: 21.2438 ± 0.0015 Å
• α: 90°
• β: 102.919 ± 0.002°
• γ: 90°
• Cell volume: 3766.4 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1585
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.1073
• Weighted residual factors for all reflections included in the refinement: 0.1147
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No