Information card for entry 4314225

Structure parameters

• Formula: K10 O45.75 Si W9
• Calculated formula: K10 O45.75 Si W9
• Title of publication: Cation-Directed Synthesis of Tungstosilicates. 1. Syntheses and Structures of K10A-α-[SiW9O34].24H2O, of the Sandwich-Type Complex K10.75[Co(H2O)6]0.5[Co(H2O)4Cl]0.25A-α-[K2{Co(H2O)2}3(SiW9O34)2].32H2O and of Cs15[K(SiW11O39)2].39H2O
• Authors of publication: Nathalie Laronze; Jérôme Marrot; Gilbert Hervé
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 5857 - 5862
• a: 33.7316 ± 0.0013 Å
• b: 16.5324 ± 0.0006 Å
• c: 17.2177 ± 0.0006 Å
• α: 90°
• β: 103.479 ± 0.001°
• γ: 90°
• Cell volume: 9337.2 ± 0.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.076
• Residual factor for significantly intense reflections: 0.0457
• Weighted residual factors for significantly intense reflections: 0.0937
• Weighted residual factors for all reflections included in the refinement: 0.1049
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No