Information card for entry 4314253

Structure parameters

• Formula: C25 H28 Cl3 N6 O3 P S
• Calculated formula: C25 H28 Cl3 N6 O3 P S
• SMILES: CN(/N=C/c1c(cccc1)O)P(N(C)/N=C/c1c(cccc1)O)(N(C)/N=C/c1c(cccc1)O)=S.C(Cl)(Cl)Cl
• Title of publication: A Phosphorus Supported Multisite Coordinating Tris Hydrazone P(S)[N(Me)NCHC6H4-o-OH]3 as an Efficient Ligand for the Assembly of Trinuclear Metal Complexes: Synthesis, Structure, and Magnetism
• Authors of publication: Vadapalli Chandrasekhar; Ramachandran Azhakar; Gurusamy Thanagavelu Senthil Andavan; Venkatasubbaiah Krishnan; Stefano Zacchini; Jamie F. Bickley; Alexander Steiner; Raymond J. Butcher; Paul Kögerler
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 5989 - 5998
• a: 10.184 ± 0.002 Å
• b: 10.895 ± 0.002 Å
• c: 14.143 ± 0.003 Å
• α: 96.83 ± 0.03°
• β: 107.19 ± 0.03°
• γ: 100.3 ± 0.03°
• Cell volume: 1450.1 ± 0.6 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0724
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.1374
• Weighted residual factors for all reflections included in the refinement: 0.1515
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No