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Information card for entry 4314292
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Coordinates | 4314292.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | tetrakis(THF)lithium-tris-3,5-dichlorophenylformamdinate vanadium(II) |
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Formula | C55 H53 Cl12 Li N6 O4 V |
Calculated formula | C55 H53 Cl12 Li N6 O4 V |
Title of publication | New Chemistry of the Triply Bonded Divanadium (V24+) Unit and Reduction to an Unprecedented V23+ Core |
Authors of publication | F. Albert Cotton; Elizabeth A. Hillard; Carlos A. Murillo; Xiaoping Wang |
Journal of publication | Inorganic Chemistry |
Year of publication | 2003 |
Journal volume | 42 |
Pages of publication | 6063 - 6070 |
a | 11.0014 ± 0.0007 Å |
b | 15.975 ± 0.001 Å |
c | 18.9046 ± 0.0012 Å |
α | 98.468 ± 0.001° |
β | 96.081 ± 0.001° |
γ | 105.737 ± 0.001° |
Cell volume | 3125.7 ± 0.3 Å3 |
Cell temperature | 213 ± 2 K |
Ambient diffraction temperature | 213 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0904 |
Residual factor for significantly intense reflections | 0.0544 |
Weighted residual factors for significantly intense reflections | 0.1338 |
Weighted residual factors for all reflections included in the refinement | 0.1532 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.014 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4314292.html
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