Crystallography Open Database

Information card for entry 4314334

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Coordinates	4314334.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H20 Cl N2 O4 Re
Calculated formula	C12 H19 Cl N2 O4 Re
Title of publication	Synthesis and Characterization of Novel Rhenium(V) Tetradentate N2O2 Schiff Base Monomer and Dimer Complexes
Authors of publication	Paul D. Benny; Charles L. Barnes; Pamela M. Piekarski; John D. Lydon; Silvia S. Jurisson
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	6519 - 6527
a	7.2888 ± 0.0006 Å
b	9.8299 ± 0.0008 Å
c	10.8195 ± 0.0009 Å
α	81.767 ± 0.001°
β	77.151 ± 0.001°
γ	87.62 ± 0.001°
Cell volume	747.96 ± 0.11 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0392
Residual factor for significantly intense reflections	0.0381
Weighted residual factors for significantly intense reflections	0.1075
Weighted residual factors for all reflections included in the refinement	0.1084
Goodness-of-fit parameter for all reflections included in the refinement	1.08
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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