Information card for entry 4314496

Structure parameters

• Formula: H50 K12 O107 Si2 W22 Zr2
• Calculated formula: K11.108 O117 Si2 W22 Zr2
• Title of publication: Peroxo-Zr/Hf-Containing Undecatungstosilicates and -Germanates
• Authors of publication: Sib Sankar Mal; Nadeen H. Nsouli; Mauro Carraro; Andrea Sartorel; Gianfranco Scorrano; Holger Oelrich; Lorenz Walder; Marcella Bonchio; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 7 - 9
• a: 11.5163 ± 0.0013 Å
• b: 12.4128 ± 0.0013 Å
• c: 21.326 ± 0.003 Å
• α: 80.355 ± 0.006°
• β: 87.259 ± 0.007°
• γ: 63.1 ± 0.005°
• Cell volume: 2678.9 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0724
• Residual factor for significantly intense reflections: 0.0557
• Weighted residual factors for significantly intense reflections: 0.1491
• Weighted residual factors for all reflections included in the refinement: 0.162
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No