Information card for entry 4314498

Structure parameters

• Formula: H42 Hf2 K10.5 O103 Rb1.5 Si2 W22
• Calculated formula: Hf2 K10.5 O103 Rb1.5 Si2 W22
• Title of publication: Peroxo-Zr/Hf-Containing Undecatungstosilicates and -Germanates
• Authors of publication: Sib Sankar Mal; Nadeen H. Nsouli; Mauro Carraro; Andrea Sartorel; Gianfranco Scorrano; Holger Oelrich; Lorenz Walder; Marcella Bonchio; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 7 - 9
• a: 11.5111 ± 0.0006 Å
• b: 12.5996 ± 0.0007 Å
• c: 19.0734 ± 0.0009 Å
• α: 91.487 ± 0.003°
• β: 92.993 ± 0.003°
• γ: 103.241 ± 0.003°
• Cell volume: 2687.1 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0679
• Residual factor for significantly intense reflections: 0.0493
• Weighted residual factors for significantly intense reflections: 0.1369
• Weighted residual factors for all reflections included in the refinement: 0.1521
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No