Information card for entry 4314527

Structure parameters

• Formula: C28 H58 Cl2 N8 Ni2 O12
• Calculated formula: C28 H58 Cl2 N8 Ni2 O12
• Title of publication: Copper(II) and Nickel(II) Complexes of β-Aminoketoxime Ligand: Syntheses, Crystal Structures, Magnetism, and Nickel(II) Templated Coupling of Oxime with Nitrile
• Authors of publication: Oindrila Das; N. N. Adarsh; Ankan Paul; Tapan Kanti Paine
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 541 - 551
• a: 20.444 ± 0.005 Å
• b: 14.148 ± 0.003 Å
• c: 16.923 ± 0.004 Å
• α: 90°
• β: 104.958 ± 0.006°
• γ: 90°
• Cell volume: 4729 ± 1.9 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0731
• Residual factor for significantly intense reflections: 0.0528
• Weighted residual factors for significantly intense reflections: 0.1442
• Weighted residual factors for all reflections included in the refinement: 0.1581
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No