Information card for entry 4314611

Structure parameters

• Formula: C15 H23 Br N2 Si
• Calculated formula: C15 H23 Br N2 Si
• Title of publication: Reactivity of a Disilylene [{PhC(NBut)2}Si]2 toward Bromine: Synthesis and Characterization of a Stable Monomeric Bromosilylene
• Authors of publication: Hui-Xian Yeong; Kai-Chung Lau; Hong-Wei Xi; Kok Hwa Lim; Cheuk-Wai So
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 371 - 373
• a: 14.2389 ± 0.0011 Å
• b: 11.1641 ± 0.0008 Å
• c: 11.9823 ± 0.0009 Å
• α: 90°
• β: 116.28 ± 0.004°
• γ: 90°
• Cell volume: 1707.9 ± 0.2 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0957
• Residual factor for significantly intense reflections: 0.0636
• Weighted residual factors for significantly intense reflections: 0.1665
• Weighted residual factors for all reflections included in the refinement: 0.1899
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No