Information card for entry 4314722

Structure parameters

• Formula: C24 H56 N2 P4 Pb Te4
• Calculated formula: C24 H56 N2 P4 Pb Te4
• Title of publication: Synthesis, Structures, and Multinuclear NMR Spectra of Tin(II) and Lead(II) Complexes of Tellurium-Containing Imidodiphosphinate Ligands: Preparation of Two Morphologies of Phase-Pure PbTe from a Single-Source Precursor
• Authors of publication: Jamie S. Ritch; Tristram Chivers; Kibriya Ahmad; Mohammad Afzaal; Paul O'Brien
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 1198 - 1205
• a: 34.833 ± 0.007 Å
• b: 9.795 ± 0.002 Å
• c: 26.044 ± 0.005 Å
• α: 90°
• β: 120.25 ± 0.03°
• γ: 90°
• Cell volume: 7676 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0461
• Residual factor for significantly intense reflections: 0.0345
• Weighted residual factors for significantly intense reflections: 0.0778
• Weighted residual factors for all reflections included in the refinement: 0.0825
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No