Information card for entry 4314735

Structure parameters

• Formula: C69 H96 Cl7 Co2 N4 O6 Si2
• Calculated formula: C69 H96 Cl7 Co2 N4 O6 Si2
• Title of publication: Lewis-Base-Stabilized Dichlorosilylene: A Two-Electron σ-Donor Ligand
• Authors of publication: Jianfeng Li; Sebastian Merkel; Julian Henn; Kathrin Meindl; Alexander Döring; Herbert W. Roesky; Rajendra S. Ghadwal; Dietmar Stalke
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 775 - 777
• a: 9.991 ± 0.0015 Å
• b: 29.253 ± 0.004 Å
• c: 25.866 ± 0.004 Å
• α: 90°
• β: 94.831 ± 0.002°
• γ: 90°
• Cell volume: 7532.9 ± 1.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0592
• Residual factor for significantly intense reflections: 0.0539
• Weighted residual factors for significantly intense reflections: 0.1244
• Weighted residual factors for all reflections included in the refinement: 0.1271
• Goodness-of-fit parameter for all reflections included in the refinement: 1.127
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No