Information card for entry 4314831

Structure parameters

• Formula: C34 H52 N2 S U
• Calculated formula: C34 H52 N2 S U
• Title of publication: Reaction Chemistry of the U3+ Metallocene Amidinate (C5Me5)2[iPrNC(Me)NiPr]U Including the Isolation of a Uranium Complex of a Monodentate Acetate
• Authors of publication: William J. Evans; Justin R. Walensky; Joseph W. Ziller
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 1743 - 1749
• a: 11.5156 ± 0.0006 Å
• b: 17.1703 ± 0.0009 Å
• c: 16.0926 ± 0.0008 Å
• α: 90°
• β: 90.232 ± 0.001°
• γ: 90°
• Cell volume: 3181.9 ± 0.3 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0344
• Residual factor for significantly intense reflections: 0.0295
• Weighted residual factors for significantly intense reflections: 0.0605
• Weighted residual factors for all reflections included in the refinement: 0.0622
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No