Information card for entry 4315127

Structure parameters

• Chemical name: methyltrichlorosilane 1,10-phenanthroline complex, THF solvate
• Formula: C17 H19 Cl3 N2 O Si
• Calculated formula: C17 H19 Cl3 N2 O Si
• Title of publication: Reactions of Hydridochlorosilanes with 2,2'-Bipyridine and 1,10-Phenanthroline: Complexation versus Dismutation and Metal-Catalyst-Free 1,4-Hydrosilylation
• Authors of publication: Gerrit W. Fester; Jana Eckstein; Daniela Gerlach; Jörg Wagler; Erica Brendler; Edwin Kroke
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 2667 - 2673
• a: 10.253 ± 0.002 Å
• b: 10.967 ± 0.002 Å
• c: 15.886 ± 0.003 Å
• α: 90°
• β: 90.316 ± 0.008°
• γ: 90°
• Cell volume: 1786.3 ± 0.6 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0917
• Residual factor for significantly intense reflections: 0.0618
• Weighted residual factors for significantly intense reflections: 0.1141
• Weighted residual factors for all reflections included in the refinement: 0.1225
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No