Crystallography Open Database

Information card for entry 4315158

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Coordinates	4315158.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H97 B2 Er2 N15 Si6
Calculated formula	C48 H97 B2 Er2 N15 Si6
Title of publication	γ-Deprotonation of Anionic Bis(trimethylsilyl)amidolanthanide Complexes with a Countered [(TpMe2)2Ln]+ Cation
Authors of publication	Fuyan Han; Jie Zhang; Weiyin Yi; Zhengxing Zhang; Jingyi Yu; Linhong Weng; Xigeng Zhou
Journal of publication	Inorganic Chemistry
Year of publication	2010
Journal volume	49
Pages of publication	2793 - 2798
a	13.284 ± 0.016 Å
b	14.543 ± 0.017 Å
c	19.62 ± 0.02 Å
α	93.049 ± 0.017°
β	95.77 ± 0.016°
γ	102.479 ± 0.016°
Cell volume	3671 ± 7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1328
Residual factor for significantly intense reflections	0.0777
Weighted residual factors for significantly intense reflections	0.1997
Weighted residual factors for all reflections included in the refinement	0.2154
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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