Information card for entry 4316094

Structure parameters

• Common name: [k-crypt]3[Ge10Mn(CO)4].tol
• Formula: C65 H116 Ge10 K3 Mn N6 O22
• Calculated formula: C65 H116 Ge10 K3 Mn N6 O22
• Title of publication: The Elusivecloso-Ge102-Zintl Ion: Finally "Captured" as a Ligand in the Complex [Ge10Mn(CO)4]3-
• Authors of publication: Daniel Rios; Slavi C. Sevov
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 6396 - 6398
• a: 15.3123 ± 0.0006 Å
• b: 20.9401 ± 0.0008 Å
• c: 28.0514 ± 0.0011 Å
• α: 90°
• β: 92.818 ± 0.002°
• γ: 90°
• Cell volume: 8983.6 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0656
• Residual factor for significantly intense reflections: 0.0412
• Weighted residual factors for significantly intense reflections: 0.0951
• Weighted residual factors for all reflections included in the refinement: 0.1053
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No