Information card for entry 4316199

Structure parameters

• Formula: C16 H38.11 Cl2 N4.95 O10 Rh
• Calculated formula: C16 H38.12 Cl2 N4.94 O10 Rh
• Title of publication: Preparation, Crystal Structure, and Unusually Facile Redox Chemistry of a Macrocyclic Nitrosylrhodium Complex
• Authors of publication: Kathleen E. Kristian; Wenjing Song; Arkady Ellern; Ilia A. Guzei; Andreja Bakac
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 7182 - 7187
• a: 7.965 ± 0.003 Å
• b: 15.393 ± 0.004 Å
• c: 10.327 ± 0.004 Å
• α: 90°
• β: 102.78 ± 0.02°
• γ: 90°
• Cell volume: 1234.8 ± 0.7 ų
• Cell temperature: 102 ± 2 K
• Ambient diffraction temperature: 102 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0378
• Residual factor for significantly intense reflections: 0.0376
• Weighted residual factors for significantly intense reflections: 0.1337
• Weighted residual factors for all reflections included in the refinement: 0.1338
• Goodness-of-fit parameter for all reflections included in the refinement: 0.989
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: Cu-Kα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No