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Information card for entry 4316382
Preview
Coordinates | 4316382.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C54.5 H53 Cl3 Cu F6 P5 |
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Calculated formula | C54 H52 Cl2 Cu F6 P5 |
Title of publication | Synthesis and Structure of Intermediates in Copper-Catalyzed Alkylation of Diphenylphosphine |
Authors of publication | Matthew F. Cain; Russell P. Hughes; David S. Glueck; James A. Golen; Curtis E. Moore; Arnold L. Rheingold |
Journal of publication | Inorganic Chemistry |
Year of publication | 2010 |
Journal volume | 49 |
Pages of publication | 7650 - 7662 |
a | 10.3838 ± 0.0006 Å |
b | 12.8816 ± 0.0007 Å |
c | 21.823 ± 0.0012 Å |
α | 86.595 ± 0.001° |
β | 77.501 ± 0.001° |
γ | 69.237 ± 0.001° |
Cell volume | 2664.3 ± 0.3 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0688 |
Residual factor for significantly intense reflections | 0.0593 |
Weighted residual factors for significantly intense reflections | 0.1443 |
Weighted residual factors for all reflections included in the refinement | 0.1489 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.044 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4316382.html
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