Information card for entry 4316461

Structure parameters

• Formula: C30 H72 N3 Na O7 Si6 U
• Calculated formula: C30 H72 N3 Na O7 Si6 U
• SMILES: [U]12([O]([Na]3456[O]7CC[O]3CC[O]4CC[O]5CC[O]6CC7)C(=C)[Si](N1[Si](C)(C)C)(C)C)(OC(=C)[Si](N2[Si](C)(C)C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: The Bis Metallacyclic Anion [U(N{SiMe3}2)(CH2SiMe2N{SiMe3})2]-
• Authors of publication: Olivier Bénaud; Jean-Claude Berthet; Pierre Thuéry; Michel Ephritikhine
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 8117 - 8130
• a: 36.9607 ± 0.0019 Å
• b: 11.0587 ± 0.0005 Å
• c: 24.2187 ± 0.0011 Å
• α: 90°
• β: 103.147 ± 0.003°
• γ: 90°
• Cell volume: 9639.6 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1154
• Residual factor for significantly intense reflections: 0.0594
• Weighted residual factors for significantly intense reflections: 0.1304
• Weighted residual factors for all reflections included in the refinement: 0.1442
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No