Crystallography Open Database

Information card for entry 4316561

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Coordinates	4316561.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C128 N8 O74 Si2 W20 Zn4
Calculated formula	C128.016 N8 O74 Si2 W20 Zn4
Title of publication	Sandwich-Type Zinc-Containing Polyoxometalates with a Hexaprismane Core [{Zn2W(O)O3}2]4+ Synthesized by Thermally Induced Isomerization of a Metastable Polyoxometalate
Authors of publication	Yuji Kikukawa; Kazuya Yamaguchi; Noritaka Mizuno
Journal of publication	Inorganic Chemistry
Year of publication	2010
Journal volume	49
Pages of publication	8194 - 8196
a	34.7252 ± 0.0004 Å
b	26.3949 ± 0.0005 Å
c	27.7763 ± 0.0006 Å
α	90°
β	119.036 ± 0.001°
γ	90°
Cell volume	22259.1 ± 0.7 Å³
Cell temperature	153 K
Ambient diffraction temperature	153 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.0777
Weighted residual factors for all reflections included in the refinement	0.2444
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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