Information card for entry 4316859

Structure parameters

• Common name: Compound 9
• Formula: C92 H108 Ge2 N4 O2 S2 Si6
• Calculated formula: C92 H108 Ge2 N4 O2 S2 Si6
• Title of publication: Low-Coordinate Germylene and Stannylene Heterocycles featuring Sterically Tunable Bis(amido)silyl Ligands
• Authors of publication: S. M. Ibrahim Al-Rafia; Paul A. Lummis; Michael J. Ferguson; Robert McDonald; Eric Rivard
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 9709 - 9717
• a: 11.766 ± 0.002 Å
• b: 13.955 ± 0.003 Å
• c: 15.759 ± 0.003 Å
• α: 65.862 ± 0.002°
• β: 72.296 ± 0.002°
• γ: 71.013 ± 0.002°
• Cell volume: 2188.5 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0331
• Residual factor for significantly intense reflections: 0.0313
• Weighted residual factors for significantly intense reflections: 0.0888
• Weighted residual factors for all reflections included in the refinement: 0.0903
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No