Information card for entry 4317004

Structure parameters

• Formula: C29 H43.31 Cl0.23 Ge N3.54
• Calculated formula: C29 H43.31 Cl0.23 Ge N3.54
• Title of publication: Correction to Synthesis and Reaction of Monomeric Germanium(II) and Lead(II) Dimethylamide and the Synthesis of Germanium(II) Hydrazide by Cleavage of One N-H Bond of Hydrazine
• Authors of publication: Anukul Jana; Herbert W. Roesky; Carola Schulzke; Prinson P. Samuel; Alexander Döring
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 10208 - 10209
• a: 8.6062 ± 0.0017 Å
• b: 11.553 ± 0.002 Å
• c: 15.055 ± 0.003 Å
• α: 97.44 ± 0.03°
• β: 98.64 ± 0.03°
• γ: 106.2 ± 0.03°
• Cell volume: 1397.8 ± 0.6 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0512
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.0982
• Weighted residual factors for all reflections included in the refinement: 0.1024
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No