Information card for entry 4317106

Structure parameters

• Formula: C8 H14 O13 Pb6
• Calculated formula: C8 H14 O13 Pb6
• Title of publication: Synthesis and Structures of Pb3O2(CH3COO)2.0.5H2O and Pb2O(HCOO)2: Two Corrosion Products Revisited
• Authors of publication: Catherine M. Mauck; Titus W. P. van den Heuvel; Michaela M. Hull; Matthias Zeller; Catherine M. Oertel
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 10736 - 10743
• a: 7.2427 ± 0.0009 Å
• b: 11.5314 ± 0.0015 Å
• c: 13.5236 ± 0.0018 Å
• α: 112.322 ± 0.002°
• β: 101.107 ± 0.002°
• γ: 90.74 ± 0.002°
• Cell volume: 1020.6 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0668
• Residual factor for significantly intense reflections: 0.0374
• Weighted residual factors for significantly intense reflections: 0.0783
• Weighted residual factors for all reflections included in the refinement: 0.0896
• Goodness-of-fit parameter for all reflections included in the refinement: 0.993
• Diffraction radiation wavelength: 0.7749 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No