Information card for entry 4317248

Structure parameters

• Formula: C184 H122 Mo2 N8 O42 Si W12
• Calculated formula: C184 H120 Mo2 N8 O42 Si W12
• Title of publication: Crystal Structures and Solution Properties of Discrete Complexes Composed of Saddle-Distorted Molybdenum(V)-Dodecaphenylporphyrins and Keggin-Type Heteropolyoxometalates Linked by Direct Coordination
• Authors of publication: Atsutoshi Yokoyama; Takahiko Kojima; Kei Ohkubo; Shunichi Fukuzumi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 11190 - 11198
• a: 18.4212 ± 0.0011 Å
• b: 37.5328 ± 0.0017 Å
• c: 17.8126 ± 0.0011 Å
• α: 90°
• β: 118.897 ± 0.002°
• γ: 90°
• Cell volume: 10782.2 ± 1.1 ų
• Cell temperature: 123.1 K
• Number of distinct elements: 7
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for significantly intense reflections: 0.0778
• Weighted residual factors for all reflections included in the refinement: 0.1817
• Goodness-of-fit parameter for all reflections included in the refinement: 1.2
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No