Information card for entry 4317338

Structure parameters

• Formula: C61.25 H58.5 Cl0.5 Ir O2 P4 Rh Si
• Calculated formula: C61.25 H58.5 Cl0.5 Ir O2 P4 Rh Si
• Title of publication: Multiple Silicon-Hydrogen Bond Activations at Adjacent Rhodium and Iridium Centers
• Authors of publication: Md Hosnay Mobarok; Okemona Oke; Michael J. Ferguson; Robert McDonald; Martin Cowie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 11556 - 11572
• a: 23.3576 ± 0.0008 Å
• b: 19.2433 ± 0.0007 Å
• c: 24.8837 ± 0.0008 Å
• α: 90°
• β: 100.444 ± 0.0004°
• γ: 90°
• Cell volume: 10999.3 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0217
• Residual factor for significantly intense reflections: 0.0179
• Weighted residual factors for significantly intense reflections: 0.0454
• Weighted residual factors for all reflections included in the refinement: 0.0473
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No