Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4317352
Preview
Coordinates | 4317352.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C46.5 H53 Mo O3 P Pb |
---|---|
Calculated formula | C46.5 H52.5 Mo O3 P Pb |
Title of publication | Chemistry of the Oxophosphinidene Ligand. 2. Reactivity of the Anionic Complexes [MCp{P(O)R*}(CO)2]- (M = Mo, W; R* = 2,4,6-C6H2tBu3) Toward Electrophiles Based on Elements Different from Carbon. |
Authors of publication | María Alonso; M. Angeles Alvarez; M. Esther García; Miguel A. Ruiz; Hayrullo Hamidov; John C. Jeffery |
Journal of publication | Inorganic Chemistry |
Year of publication | 2010 |
Journal volume | 49 |
Pages of publication | 11595 - 11605 |
a | 55.003 ± 0.0014 Å |
b | 10.23 ± 0.0003 Å |
c | 15.0932 ± 0.0004 Å |
α | 90° |
β | 91.158 ± 0.001° |
γ | 90° |
Cell volume | 8490.9 ± 0.4 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0416 |
Residual factor for significantly intense reflections | 0.0315 |
Weighted residual factors for significantly intense reflections | 0.0762 |
Weighted residual factors for all reflections included in the refinement | 0.0806 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.034 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4317352.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.