Information card for entry 4317397

Structure parameters

• Formula: C24 H15 N4 Ni O11 V4
• Calculated formula: C24 H15 N4 Ni O11 V4
• Title of publication: Hydrothermal Synthesis and Crystal Structure of a Novel Two-Dimensional Vanadium Oxide Complex with a 6,14-Net Sinusoidal Ruffling Anionic Layer: [Ni(phen)2V4O11] (phen = 1,10-Phenanthroline)
• Authors of publication: Cai-Ming Liu; Yang-Long Hou; Jing Zhang; Song Gao
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 140 - 143
• a: 9.6518 ± 0.0002 Å
• b: 18.4585 ± 0.0004 Å
• c: 17.7056 ± 0.0004 Å
• α: 90°
• β: 95.26 ± 0.001°
• γ: 90°
• Cell volume: 3141.11 ± 0.12 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0524
• Residual factor for significantly intense reflections: 0.0383
• Weighted residual factors for significantly intense reflections: 0.0901
• Weighted residual factors for all reflections included in the refinement: 0.0979
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No