Information card for entry 4317434

Structure parameters

• Formula: C120 H110 B2 Cl6 F10 N2 P8 Re2
• Calculated formula: C120 H110 B2 Cl6 F10 N2 P8 Re2
• Title of publication: Activation of Organonitriles toward β-Electrophilic Attack. Synthesis and Characterization of Methyleneamide (Azavinylidene) Complexes of Rhenium
• Authors of publication: M. Fátima C. Guedes da Silva; João J. R. Fraústo da Silva; Armando J. L. Pombeiro
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 219 - 228
• a: 12.881 ± 0.003 Å
• b: 14.767 ± 0.003 Å
• c: 17.785 ± 0.004 Å
• α: 84.55 ± 0.02°
• β: 74.64 ± 0.02°
• γ: 65.82 ± 0.02°
• Cell volume: 2975.6 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0961
• Residual factor for significantly intense reflections: 0.067
• Weighted residual factors for significantly intense reflections: 0.1677
• Weighted residual factors for all reflections included in the refinement: 0.1908
• Goodness-of-fit parameter for all reflections included in the refinement: 1.122
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No