Information card for entry 4317504

Structure parameters

• Formula: C92 H90 N12 O8 P4 Rh2
• Calculated formula: C92 H85 N12 O8 P4 Rh2
• Title of publication: Oxidative Addition of N-H Bonds to a Metal Center: Synthesis, Characterization, and Crystal Structure of New Rhodium(III) Hydrido-Pyrazolate Complexes
• Authors of publication: G. Attilio Ardizzoia; Stefano Brenna; Girolamo LaMonica; Angelo Maspero; Norberto Masciocchi; Massimo Moret
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 610 - 614
• a: 12.537 ± 0.002 Å
• b: 18.113 ± 0.003 Å
• c: 38.231 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8682 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P b n 21
• Hall space group symbol: P 2c -2ab
• Residual factor for all reflections: 0.0472
• Residual factor for significantly intense reflections: 0.0472
• Weighted residual factors for significantly intense reflections: 0.0896
• Weighted residual factors for all reflections included in the refinement: 0.0896
• Goodness-of-fit parameter for all reflections included in the refinement: 1.124
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No