Information card for entry 4317536

Structure parameters

• Common name: PbPh2Cl2.[VO(3-MeOsalen).H2O]
• Chemical name: Diphenyllead dichloride.[N,N'-bis(3-methoxysalicylidene)ethane-1,2-diaminato]monoaq ua oxovanadium(IV) (1/1)
• Formula: C31 H30 Cl4 N2 O6 Pb V
• Calculated formula: C31 H30 Cl4 N2 O6 Pb V
• SMILES: [Pb](Cl)(Cl)(O[V]123(Oc4c(OC)cccc4C=[N]2CC[N]3=Cc2cccc(OC)c2O1)[OH2])(c1ccccc1)c1ccccc1.ClCCl
• Title of publication: Donor Properties of the Vanadyl Ion: Reactions of Vanadyl Salicylaldimine β-Ketimine and Acetylacetonato Complexes with Groups 14 and 15 Lewis Acids
• Authors of publication: B. Cashin; D. Cunningham; P. Daly; P. McArdle; M. Munroe; N. Ní Chonchubhair
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 773 - 782
• a: 11.7273 ± 0.0014 Å
• b: 13.1533 ± 0.0018 Å
• c: 13.295 ± 0.005 Å
• α: 99.9 ± 0.02°
• β: 113.7 ± 0.02°
• γ: 105.235 ± 0.011°
• Cell volume: 1720.1 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1921
• Residual factor for significantly intense reflections: 0.171
• Weighted residual factors for significantly intense reflections: 0.3825
• Weighted residual factors for all reflections included in the refinement: 0.4029
• Goodness-of-fit parameter for all reflections included in the refinement: 1.74
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No