Information card for entry 4317579

Structure parameters

• Formula: C79.5 H65 Cl Hg2 O P4 Pd
• Calculated formula: C79.5 H64 Cl Hg2 O P4 Pd
• Title of publication: Bis{(2-diphenylphosphino)phenyl}mercury: A P-Donor Ligand and Precursor to Mixed Metal-Mercury (d8-d10) Cyclometalated Complexes Containing 2-C6H4PPh2
• Authors of publication: Martin A. Bennett; Maria Contel; David C. R. Hockless; Lee L. Welling; Anthony C. Willis
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 844 - 855
• a: 13.199 ± 0.001 Å
• b: 15.273 ± 0.002 Å
• c: 17.85 ± 0.001 Å
• α: 93.83 ± 0.007°
• β: 93.664 ± 0.006°
• γ: 104.378 ± 0.007°
• Cell volume: 3465.8 ± 0.6 ų
• Cell temperature: 193.2 K
• Ambient diffraction temperature: 193.2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0418
• Residual factor for significantly intense reflections: 0.0305
• Weighted residual factors for all reflections: 0.0339
• Weighted residual factors for all reflections included in the refinement: 0.0326
• Goodness-of-fit parameter for all reflections: 1.784
• Goodness-of-fit parameter for all reflections included in the refinement: 1.89
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No