Information card for entry 4317684

Structure parameters

• Formula: C45 H54 Cl15 N9 Sb2
• Calculated formula: C45 H54 Cl15 N9 Sb2
• Title of publication: Structures of Sb(OC6H3Me2-2,6)3 and Sb(OEt)5.NH3: The First Authenticated Monomeric Sb(OR)n (n= 3, 5)
• Authors of publication: Graeme A. Horley; Mary F. Mahon; Kieran C. Molloy; Monica M. Venter; Peter W. Haycock; Christopher P. Myers
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 1652 - 1657
• a: 13.43 ± 0.0002 Å
• b: 14.418 ± 0.0002 Å
• c: 17.418 ± 0.0003 Å
• α: 82.765 ± 0.0007°
• β: 77.557 ± 0.0007°
• γ: 70.767 ± 0.0007°
• Cell volume: 3104.14 ± 0.08 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0842
• Residual factor for significantly intense reflections: 0.0417
• Weighted residual factors for significantly intense reflections: 0.1035
• Weighted residual factors for all reflections included in the refinement: 0.1281
• Goodness-of-fit parameter for all reflections included in the refinement: 0.844
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No