Information card for entry 4317877

Structure parameters

• Formula: C52 H72 F21 Li5 N8 Si8
• Calculated formula: C52 H72 F21 Li5 N8 Si8
• SMILES: C1(c2c(F)c(F)c(F)c(F)c2F)=[N]2([Si](C)(C)C)[Li]34[N](=C5c6c(F)c(F)c(F)c(F)c6F)([Si](C)(C)C)[Li]6([N]35[Si](C)(C)C)[N](=C3c5c(F)c(F)c(F)c(F)c5F)([Si](C)(C)C)[Li]57[N]3([Si](C)(C)C)[Li]38[N]5([Si](C)(C)C)=C([N]3([Si](C)(C)C)[Li]2([N]1[Si](C)(C)C)[F]4678)c1c(F)c(F)c(F)c(F)c1F
• Title of publication: Lithium Fluoroarylamidinates: Syntheses, Structures, and Reactions
• Authors of publication: Carsten Knapp; Enno Lork; Paul G. Watson; Rüdiger Mews
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 2014 - 2025
• a: 26.192 ± 0.004 Å
• b: 10.545 ± 0.003 Å
• c: 26.954 ± 0.004 Å
• α: 90°
• β: 99.33 ± 0.01°
• γ: 90°
• Cell volume: 7346 ± 3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1876
• Residual factor for significantly intense reflections: 0.0754
• Weighted residual factors for significantly intense reflections: 0.117
• Weighted residual factors for all reflections included in the refinement: 0.1516
• Goodness-of-fit parameter for all reflections included in the refinement: 0.972
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No