Information card for entry 4317948

Structure parameters

• Formula: C54 H50 Ag B3 Cl4 F4 N12 P2 Rh2
• Calculated formula: C54 H50 Ag B3 Cl4 F4 N12 P2 Rh2
• Title of publication: Synthesis and Molecular Structure of [{(HBpz3)Rh(PPh3)(μ-Cl)2}2Ag]BF4 (Hpz = Pyrazole), a Heterotrinuclear Rh2Ag Compound with Square-Planar Silver(I)
• Authors of publication: Daniel Carmona; Fernando Viguri; Fernando J. Lahoz; Luis A. Oro
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 2385 - 2388
• a: 24.329 ± 0.004 Å
• b: 10.3786 ± 0.0015 Å
• c: 23.883 ± 0.004 Å
• α: 90°
• β: 91.262 ± 0.015°
• γ: 90°
• Cell volume: 6029 ± 1.7 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 9
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1114
• Residual factor for significantly intense reflections: 0.0542
• Weighted residual factors for significantly intense reflections: 0.1097
• Weighted residual factors for all reflections included in the refinement: 0.1285
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No