Information card for entry 4317968

Structure parameters

• Chemical name: bis{[bis(2-hydroxyiminopropyl)(μ-N,O-2-oxyiminopropyl)amine] acetonitrilo nickel(II)} bis(perchlorate)
• Formula: C22 H40 Cl2 N10 Ni2 O14
• Calculated formula: C22 H40 Cl2 N10 Ni2 O14
• Title of publication: Oxygen Reactivity of a Nickel(II)-Polyoximate Complex
• Authors of publication: Michael J. Goldcamp; Sara E. Robison; Jeanette A. Krause Bauer; Michael J. Baldwin
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 2307 - 2309
• a: 8.233 ± 0.002 Å
• b: 21.83 ± 0.004 Å
• c: 9.703 ± 0.002 Å
• α: 90°
• β: 94.04 ± 0.003°
• γ: 90°
• Cell volume: 1739.6 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1515
• Residual factor for significantly intense reflections: 0.0638
• Weighted residual factors for significantly intense reflections: 0.1166
• Weighted residual factors for all reflections included in the refinement: 0.1468
• Goodness-of-fit parameter for all reflections included in the refinement: 1.116
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No