Information card for entry 4318221

Structure parameters

• Formula: C47.5 H23 Cl O22 Os6 P4
• Calculated formula: C47.25 H22 Cl0.5 O22 Os6 P4
• Title of publication: 1,2,3,4-Tetraphenyl-1,2,3,4-tetraphospholane, a Highly Versatile Cyclocarbaphosphine Ligand: Reactions with Activated Triosmium Clusters and Characterization of the Products
• Authors of publication: Siau-Gek Ang; Zhong; How-Ghee Ang
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 3791 - 3800
• a: 12.2713 ± 0.0002 Å
• b: 37.622 ± 0.0006 Å
• c: 25.1179 ± 0.0001 Å
• α: 90°
• β: 96.053 ± 0.001°
• γ: 90°
• Cell volume: 11531.6 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1
• Residual factor for significantly intense reflections: 0.0583
• Weighted residual factors for significantly intense reflections: 0.1105
• Weighted residual factors for all reflections included in the refinement: 0.125
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No