Information card for entry 4318229

Structure parameters

• Formula: C12 H21.2 K4 O23.6 V2
• Calculated formula: C12 H15 K4 O23.6 V2
• Title of publication: A New Dinuclear Vanadium(V)-Citrate Complex from Aqueous Solutions. Synthetic, Structural, Spectroscopic, and pH-Dependent Studies in Relevance to Aqueous Vanadium(V)-Citrate Speciation
• Authors of publication: M. Kaliva; T. Giannadaki; A. Salifoglou; C. P. Raptopoulou; A. Terzis
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 3850 - 3858
• a: 11.093 ± 0.004 Å
• b: 9.186 ± 0.003 Å
• c: 15.503 ± 0.005 Å
• α: 78.6 ± 0.01°
• β: 86.16 ± 0.01°
• γ: 69.87 ± 0.01°
• Cell volume: 1454 ± 0.9 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.051
• Weighted residual factors for all reflections: 0.1442
• Weighted residual factors for significantly intense reflections: 0.1392
• Goodness-of-fit parameter for all reflections: 1.063
• Goodness-of-fit parameter for significantly intense reflections: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No