Information card for entry 4318279

Structure parameters

• Common name: NacNacCoCl2Li(thf)2*1.5 toluene
• Formula: C47.5 H67.5 Cl2 Co Li N2 O2
• Calculated formula: C47.5 H67.5 Cl2 Co Li N2 O2
• Title of publication: Synthesis and Characterization of Three-Coordinate and Related β-Diketiminate Derivatives of Manganese, Iron, and Cobalt
• Authors of publication: Arunashree Panda; Matthias Stender; Robert J. Wright; Marilyn M. Olmstead; Peter Klavins; Philip P. Power
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 3909 - 3916
• a: 16.4549 ± 0.0011 Å
• b: 17.8271 ± 0.0012 Å
• c: 15.8304 ± 0.0011 Å
• α: 90°
• β: 91.486 ± 0.001°
• γ: 90°
• Cell volume: 4642.2 ± 0.5 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0572
• Residual factor for significantly intense reflections: 0.0394
• Weighted residual factors for significantly intense reflections: 0.0966
• Weighted residual factors for all reflections included in the refinement: 0.1047
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No