Information card for entry 4318319

Structure parameters

• Formula: O11 Rb2 Si4 V
• Calculated formula: O11.12 Rb2 Si4 V
• Title of publication: High-Temperature, High-Pressure Hydrothermal Synthesis, Crystal Structure, and Solid State NMR Spectroscopy of a New Vanadium(IV) Silicate: Rb2(VO)(Si4O10).xH2O
• Authors of publication: Chun-Yi Li; Chan-Yen Hsieh; Hsiu-Mei Lin; Hsien-Ming Kao; Kwang-Hwa Lii
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4206 - 4210
• a: 12.2225 ± 0.0007 Å
• b: 12.2225 ± 0.0007 Å
• c: 7.7948 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1164.46 ± 0.13 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 4
• Space group number: 109
• Hermann-Mauguin space group symbol: I 41 m d
• Hall space group symbol: I 4bw -2
• Residual factor for all reflections: 0.0292
• Residual factor for significantly intense reflections: 0.0286
• Weighted residual factors for significantly intense reflections: 0.0721
• Weighted residual factors for all reflections included in the refinement: 0.0723
• Goodness-of-fit parameter for all reflections included in the refinement: 1.133
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No