Information card for entry 4318328

Structure parameters

• Formula: C10 H17 Cl4 N3 V
• Calculated formula: C10 H17 Cl4 N3 V
• SMILES: c1(c(cccc1Cl)Cl)N=[V]([NH](C)C)([NH](C)C)(Cl)Cl
• Title of publication: Synthesis and Structure of a Series of New d1-Aryl Imido-Vanadium(IV) Complexes Stabilized by N-Donor Ligands
• Authors of publication: Christian Lorber; Robert Choukroun; Bruno Donnadieu
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4217 - 4226
• a: 9.879 ± 0.005 Å
• b: 10.247 ± 0.005 Å
• c: 10.334 ± 0.005 Å
• α: 109.261 ± 0.005°
• β: 100.005 ± 0.005°
• γ: 117.271 ± 0.005°
• Cell volume: 809.3 ± 0.7 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0683
• Residual factor for significantly intense reflections: 0.0586
• Weighted residual factors for significantly intense reflections: 0.1504
• Weighted residual factors for all reflections included in the refinement: 0.1587
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No