Information card for entry 4318331

Structure parameters

• Formula: C19 H22 Cl4 N4 V
• Calculated formula: C19 H22 Cl4 N4 V
• SMILES: [V]1(Cl)(Cl)(=Nc2ccccc2)([n]2ccccc2c2[n]1cccc2)[NH](C)C.C(Cl)Cl
• Title of publication: Synthesis and Structure of a Series of New d1-Aryl Imido-Vanadium(IV) Complexes Stabilized by N-Donor Ligands
• Authors of publication: Christian Lorber; Robert Choukroun; Bruno Donnadieu
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4217 - 4226
• a: 9.916 ± 0.005 Å
• b: 11.723 ± 0.005 Å
• c: 12.082 ± 0.005 Å
• α: 110.152 ± 0.005°
• β: 112.847 ± 0.005°
• γ: 96.685 ± 0.005°
• Cell volume: 1163.1 ± 0.9 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0374
• Residual factor for significantly intense reflections: 0.0349
• Weighted residual factors for significantly intense reflections: 0.0918
• Weighted residual factors for all reflections included in the refinement: 0.0938
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No