Information card for entry 4318384

Structure parameters

• Formula: C50 H68 B Ir2 P2 S4 V
• Calculated formula: C50 H68 B Ir2 P2 S4 V
• Title of publication: Sulfur-Bridged Early-Late Heterobimetallics Synthesized by Incorporation of Titanium, Vanadium, and Molybdenum into Bis(hydrosulfido) Templates of Group 9 Metals
• Authors of publication: Shigeki Kuwata; Tatsuya Nagano; Akihiro Matsubayashi; Youichi Ishii; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4324 - 4330
• a: 9.639 ± 0.002 Å
• b: 17.274 ± 0.004 Å
• c: 32.559 ± 0.006 Å
• α: 82.58 ± 0.02°
• β: 83.45 ± 0.02°
• γ: 85.35 ± 0.02°
• Cell volume: 5329 ± 2 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0465
• Residual factor for significantly intense reflections: 0.0465
• Weighted residual factors for significantly intense reflections: 0.0474
• Weighted residual factors for all reflections included in the refinement: 0.0474
• Goodness-of-fit parameter for all reflections included in the refinement: 1.518
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No