Information card for entry 4318386

Structure parameters

• Formula: C87 H90 Cl3 I Ni3 O3 P6 Sn
• Calculated formula: C87 H90 Cl3 I Ni3 O3 P6 Sn
• Title of publication: Tin-Capped Trinuclear Nickel Clusters: Redox Isomerism between μ3-Stannyl and μ3-Stannylene Clusters of the Class [Ni3(dppm)3(μ3-I)(μ3-SnClx)]n+ (x= 2,n= 1;x= 3,n= 0)
• Authors of publication: Brian K. Breedlove; Philip E. Fanwick; Clifford P. Kubiak
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4306 - 4308
• a: 14.4869 ± 0.0005 Å
• b: 14.8724 ± 0.0006 Å
• c: 20.4779 ± 0.0009 Å
• α: 69.8506 ± 0.0015°
• β: 89.1702 ± 0.0015°
• γ: 78.01 ± 0.003°
• Cell volume: 4043.8 ± 0.3 ų
• Cell temperature: 149 K
• Ambient diffraction temperature: 149 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.06
• Weighted residual factors for all reflections included in the refinement: 0.14
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MO-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No