Information card for entry 4318388

Structure parameters

• Formula: C34 H26 Cl Cr N8 O4
• Calculated formula: C34 H26 Cl Cr N8 O4
• SMILES: [Cr]1234(N(c5ccccc5)c5ccccc5[N]1=Nc1[n]2cccc1)N(c1ccccc1)c1ccccc1[N]3=Nc1[n]4cccc1.Cl(=O)(=O)(=O)[O-]
• Title of publication: Chromium Complexes of an Isomeric N-Donor Ligand, 2-[(N-Arylamino)phenylazo]pyridine: Amination Reactions, X-ray Structure, and Redox Properties
• Authors of publication: Kunal K. Kamar; Amrita Saha; Alfonso Castiñeiras; Chen-Hsiung Hung; Sreebrata Goswami
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4531 - 4538
• a: 9.1815 ± 0.0012 Å
• b: 10.347 ± 0.0014 Å
• c: 17.22 ± 0.002 Å
• α: 103.975 ± 0.003°
• β: 91.119 ± 0.003°
• γ: 93.829 ± 0.003°
• Cell volume: 1582.9 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1685
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.0825
• Weighted residual factors for all reflections included in the refinement: 0.138
• Goodness-of-fit parameter for all reflections included in the refinement: 0.607
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No