Information card for entry 4318457

Structure parameters

• Formula: C24 H24 F2 Ge
• Calculated formula: C24 H24 F2 Ge
• SMILES: C(=C(C(C)(C)C)\F)(F)\[Ge](c1ccccc1)(c1ccccc1)c1ccccc1
• Title of publication: Spectroscopic and Structural Assignment of the Absolute Stereochemistry in a Series of 1,2-Difluorovinyl Organometalloids. The First Crystallographic Characterization and Structural Series of Group 14 Fluorovinyl Compounds
• Authors of publication: Alan K. Brisdon; Ian R. Crossley; Robin G. Pritchard; John E. Warren
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4748 - 4755
• a: 11.4276 ± 0.0002 Å
• b: 11.4998 ± 0.0002 Å
• c: 32.0449 ± 0.0005 Å
• α: 90°
• β: 93.797 ± 0.001°
• γ: 90°
• Cell volume: 4201.94 ± 0.12 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0792
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.0973
• Weighted residual factors for all reflections included in the refinement: 0.1111
• Goodness-of-fit parameter for all reflections included in the refinement: 0.988
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No