Information card for entry 4318464

Structure parameters

• Formula: C24 H30 Mo2 N2 Se5
• Calculated formula: C24 H30 Mo2 N2 Se5
• Title of publication: Synthesis and Reactions of Group 6 Metal Half-Sandwich Complexes of 2,2-Dicyanoethylene-1,1-dichalcogenolates [(Cp*)M{E2CC(CN)2}2]- (M = Mo, W; E = S, Se)
• Authors of publication: Maochun Hong; Rong Cao; Hiroyuki Kawaguchi; Kazuyuki Tatsumi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4824 - 4833
• a: 12.4408 ± 0.0007 Å
• b: 15.4474 ± 0.0003 Å
• c: 15.2899 ± 0.0002 Å
• α: 90°
• β: 109.875 ± 0.0004°
• γ: 90°
• Cell volume: 2763.36 ± 0.17 ų
• Cell temperature: 273.2 K
• Ambient diffraction temperature: 273.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0387
• Residual factor for significantly intense reflections: 0.0387
• Weighted residual factors for significantly intense reflections: 0.0503
• Weighted residual factors for all reflections included in the refinement: 0.0503
• Goodness-of-fit parameter for all reflections included in the refinement: 1.945
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No